Hydrazine hydrate (1:1) → 2-Amino-5-fluorobenzophenone hydrazone

HRID 267403

반응식

HRID 267403 반응식
[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH2:16])=[C:6]([CH:15]=1)[C:7]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=O.O.[NH2:18][NH2:19]>C(O)COCCO>[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH2:16])=[C:6]([CH:15]=1)[C:7](=[N:18][NH2:19])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 778082(2-Amino-5-fluorophenyl)(phenyl)methanone

생성물 1

HCID 867331112-Amino-5-fluorobenzophenone hydrazone

시약·촉매·용매 1

HCID 8117Diethylene Glycol용매

실험 절차

In the manner given in Preparation 1, 5-fluoro-2-aminobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 5-fluoro-2-aminobenzophenone hydrazone.

출처 및 근거

ORD 기록
ord-f2e072d34ba142fcb4eecc15e5ebf38d
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03941803

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