Hydrazine hydrate (1:1) → 2-Amino-2'-fluoro-5-chlorobenzophenone hydrazone

HRID 267404

반응식

HRID 267404 반응식
[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[F:12])=O.O.[NH2:19][NH2:20]>C(O)COCCO>[NH2:1][C:2]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:3]=1[C:4](=[N:19][NH2:20])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[F:12]

참가 물질

4

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 699122-Amino-5-chloro-2'-fluorobenzophenone

생성물 1

HCID 867330952-Amino-2'-fluoro-5-chlorobenzophenone hydrazone

시약·촉매·용매 1

HCID 8117Diethylene Glycol용매

실험 절차

In the manner given in Preparation 1, 2-amino-5-chloro-2'-fluorobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 2-amino-5-chloro-2'-fluorobenzophenone hydrazone.

출처 및 근거

ORD 기록
ord-e1de8da80ec74b7f8176b18993a298d3
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03941803

연결된 노트

불러오는 중…