2-Amino-4-chlorophenol → 2-Acetylamino-4-chlorophenol
반응식
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[OH:9].[C:10](OC(=O)C)(=[O:12])[CH3:11]>CO>[Cl:8][C:6]1[CH:5]=[CH:4][C:3]([OH:9])=[C:2]([NH:1][C:10](=[O:12])[CH3:11])[CH:7]=1참가 물질
4
실험 절차
To a suspension of 2-amino-4-chlorophenol (1.43 g, 10.0 mmol) in methanol was added acetic anhydride (0.945 mL, 10.0 mmol) and the reaction mixture was stirred at room temperature for 2 h. The volatiles were removed in vacuo to give the subtitled compound (1.5 g).
후처리
- customThe volatiles were removed in vacuo
출처 및 근거
- ORD 기록
- ord-40c22dff81724e1d9b69e1626f222a07
- 출처 데이터셋
- uspto-grants-2008_11
- 특허 번호
- US07449475B2
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