Dimethyl Sulfoxide → 2-{[(Ethenyloxy)carbonyl]oxy}ethyl 2-methylprop-2-enoate
반응식
[C:1](=[O:15])([O:12][CH:13]=[CH2:14])[O:2][C:3]1[CH:8]=CC([N+]([O-])=O)=CC=1.OCC[O:19][C:20](=[O:24])[C:21]([CH3:23])=[CH2:22].CS(C)=O.[OH-].[Na+]>O>[C:1](=[O:15])([O:12][CH:13]=[CH2:14])[O:2][CH2:3][CH2:8][O:24][C:20](=[O:19])[C:21]([CH3:23])=[CH2:22]참가 물질
6
실험 절차
A solution of p-nitrophenyl vinyl carbonate, hydroxyethylmethacrylate, DMSO and sodium hydroxide is stirred at room temperature for a minimum of 12 hours. Reaction completion is monitored by G.C. The solution is drowned into water and the mixture extracted with ethyl acetate. The product solution is washed with water, dried with magnesium sulfate, then stripped to an oil under vacuum. The crude product is then purified.
후처리
- customReaction completion
- extractionthe mixture extracted with ethyl acetate
- washThe product solution is washed with water
- dry with materialdried with magnesium sulfate
- customThe crude product is then purified
출처 및 근거
- ORD 기록
- ord-85135ddd2ee94013b167317a3cada355
- 출처 데이터셋
- uspto-grants-2002_03
- 특허 번호
- US06362363B1
반응 노트
불러오는 중…