Hydrochloric Acid → 2-Acetylthio-3-methylbenzoic acid
반응식
[SH:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[C:12](OC(=O)C)(=[O:14])[CH3:13].Cl>C(O)(=O)C>[C:12]([S:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:14])[CH3:13]참가 물질
5
실험 절차
2-Mercapto-3-methylbenzoic acid (9.0 g, 54 mmol), acetic anhydride (6.5 g, 63 mmol) and glacial acetic acid (25 ml) were refluxed 1 hour, then poured into dilute hydrochloric acid. The product was filtered and recrystallized from toluene.
후처리
- filtrationThe product was filtered
- customrecrystallized from toluene
출처 및 근거
- ORD 기록
- ord-6715ab2fd23843db950559761faa08af
- 출처 데이터셋
- uspto-grants-1984_04
- 특허 번호
- US04440941
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