Hydrochloric Acid → 2-Acetylthio-3-methoxybenzoic acid

HRID 325498노트

반응식

HRID 325498 반응식
[SH:1][C:2]1[C:10]([O:11][CH3:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[C:13](OC(=O)C)(=[O:15])[CH3:14].Cl>C(O)(=O)C>[C:13]([S:1][C:2]1[C:10]([O:11][CH3:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:15])[CH3:14]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 7918Acetic AnhydrideHCID 166556102-Mercapto-3-methoxybenzoic acid

생성물 1

HCID 204652112-Acetylthio-3-methoxybenzoic acid

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

A solution of 2-mercapto-3-methoxybenzoic acid (14.6 g, 79 mmol), acetic anhydride (9.7 g, 95 mmol) and glacial acetic acid (35 ml) was refluxed 15 minutes, then cooled and poured into dilute hydrochloric acid. The product was vacuum-filtered.

후처리

  1. temperaturecooled
  2. filtrationThe product was vacuum-filtered

출처 및 근거

ORD 기록
ord-30eff028606941938fb119fa7a2bed0d
출처 데이터셋
uspto-grants-1984_04
특허 번호
US04440941

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