Glycine → Magnesium Glycinate

HRID 328560

반응식

HRID 328560 반응식
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].C(=O)([O-])[O-].[Mg+2:10].[N+]([O-])([O-])=O.[OH-].[Al+3].[OH-].[OH-].S([O-])([O-])(=O)=O.[Al+3].S([O-])([O-])(=O)=O.S([O-])([O-])(=O)=O.[Al+3]>O>[NH2:1][CH2:2][C:3]([O-:5])=[O:4].[Mg+2:10].[NH2:1][CH2:2][C:3]([O-:5])=[O:4]

참가 물질

7

반응물 5

HCID 750GlycineHCID 943NitrateHCID 11029Magnesium CarbonateHCID 24850Aluminum SulfateHCID 10176082Aluminum Hydroxide

생성물 1

HCID 84645Magnesium Glycinate

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
75 °C

실험 절차

Magnesium glycinate was prepared by reacting 5 grams of glycine with 3.1 grams of basic magnesium carbonate (26.3% Mg) in 15 grams of water. The mixture was heated at 75° C. for 1/2 hour with agitation. The hot solution was then added to 113 grams of zirconyl nitrate (7.9% Zr) with stirring. After the addition of 1.5 grams of aluminum hydroxide powder (28.8% Al), the mixture was reacted with agitation at 75° C. for 1/2 hour. To the resultant clear solution was added 7.9 grams of 2/3 basic aluminum sulfate, Al(OH)2SO4 (3.1% Al). The solution was then oven dried at 58° C. under a vacuum of 328 mm of Hg. The product contained 1.2% Mg, 13.2% glycine, 1.5% Al, 24.3% Zr, 4.02% SO4 and 29.5% nitrate.

후처리

  1. customthe mixture was reacted with agitation at 75° C. for 1/2 hour
  2. customoven dried at 58° C. under a vacuum of 328 mm of Hg

출처 및 근거

ORD 기록
ord-b20a6d4cdab24044b85bc4f29bad8363
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017599

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