(3-Aminopropyl)triethoxysilane → Magnesium Acetate

HRID 333524

반응식

HRID 333524 반응식
O.O.O.O.[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11].NCCC[Si](OCC)(OCC)OCC.[SiH4].[Mg]>O>[C:5]([O-:8])(=[O:7])[CH3:6].[Mg+2:9].[C:10]([O-:13])(=[O:12])[CH3:11]

참가 물질

6

반응물 4

HCID 13521(3-Aminopropyl)triethoxysilaneHCID 23953Silane2회HCID 134717Magnesium Acetate TetrahydrateHCID 5462224Magnesium

생성물 1

HCID 8896Magnesium Acetate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

An aqueous magnesium acetate solution was prepared by adding 1.07 g of magnesium acetate tetrahydrate as a Group 2 or 3 element compound to 30 g of ion-exchanged water and then stirring this solution with a homomixer T. K. ROBOMIX (manufactured by PRIMIX Corporation). Then, 0.44 g of 3-aminopropyltriethoxysilane (KBE-903 manufactured by Shin-Etsu Chemical Co., Ltd.) as a silane coupling agent was gradually added to the aqueous solution. This mixture was subsequently stirred for 5 hours to induce hydrolysis and a condensation reaction of the silane coupling agent, thereby producing a suspension containing a composite compound which contained magnesium and silicon.

후처리

  1. stirringThis mixture was subsequently stirred for 5 hours
  2. customhydrolysis
  3. customproducing a suspension
  4. additioncontaining a composite compound which

출처 및 근거

ORD 기록
ord-95f51b42eeec48c1a080afb136811dd8
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08883276B2

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