7-Methylisatin → HCID 13519800, 화합물

HRID 371322

반응식

HRID 371322 반응식
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8](=[O:11])[C:7]2=[O:12].[Br:13]Br>ClC(Cl)C>[Br:13][CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][C:8](=[O:11])[C:7]2=[O:12]

참가 물질

4

반응물 2

HCID 143137-MethylisatinHCID 24408Bromine

생성물 1

HCID 13519800HCID 13519800, 화합물

시약·촉매·용매 1

HCID 63651,1-Dichloroethane용매

실험 절차

The 7-methylisatin (16.1 g, 0.1 mole) is suspended in dichloroethane (2000 ml) and the suspension is heated and irradiated with a high intensity light source to the reflux point. Bromine (24.3 g, 0.15 mole) is added dropwise over a one hour period.

후처리

  1. temperaturethe suspension is heated
  2. customirradiated with a high intensity light source to the reflux point

출처 및 근거

ORD 기록
ord-ff59d6552f17494db82c24337df43ee5
출처 데이터셋
uspto-grants-1985_07
특허 번호
US04530929

연결된 노트

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