Veratrole → 3,4-Dimethoxybenzophenone

HRID 378753

반응식

HRID 378753 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[O:9][CH3:10].[C:11](Cl)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[Cl-].[Al+3].[Cl-].[Cl-]>>[CH3:1][O:2][C:3]1[CH:8]=[C:7]([CH:6]=[CH:5][C:4]=1[O:9][CH3:10])[C:11]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[O:18]

참가 물질

4

반응물 3

HCID 7043VeratroleHCID 7412Benzoyl chlorideHCID 6451240Aluminum(III) Chloride

생성물 1

HCID 2867423,4-Dimethoxybenzophenone수율 95.7%

실험 절차

The process of Step 1, Example 4 was followed except that 292 grams of 1,2-dimethoxy benzene, 297 grams of benzoyl chloride, and 281 grams of aluminum chloride were used to yield 490 grams of 3,4-dimethoxy benzophenone.

출처 및 근거

ORD 기록
ord-02c47444813f491eb7b99c1d7a363f28
출처 데이터셋
uspto-grants-2001_10
특허 번호
US06296785B1

연결된 노트

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