홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Water → Calcium di(L-lysinate)

HRID 434182
노트
인쇄 미리보기

반응식

HRID 434182 반응식
[O-2].[Ca+2:2].[NH2:3][C@H:4]([C:10]([OH:12])=[O:11])[CH2:5][CH2:6][CH2:7][CH2:8][NH2:9].O>CCCCCC>[NH2:3][C@H:4]([C:10]([O-:12])=[O:11])[CH2:5][CH2:6][CH2:7][CH2:8][NH2:9].[Ca+2:2].[NH2:3][C@H:4]([C:10]([O-:12])=[O:11])[CH2:5][CH2:6][CH2:7][CH2:8][NH2:9]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 962WaterHCID 5962L-LysineHCID 6850728Calciumoxide

생성물 1

HCID 6454211Calcium di(L-lysinate)수율 99.3%

시약·촉매·용매 1

HCID 8058Hexane용매

실험 절차

5.6 grams (0.1 Mole) of calcium oxide and 29.2 grams (0.2 Mole) of lysine were placed into a beaker provided with a reflux condenser and a Dean Stark water trap. 100 ml hexane was added and the mixture was stirred and boiled at atmospheric pressure for 5 hours. The reaction mixture was cooled, and was thereafter filtered yielding 32.8 grams of calcium lysinate having the physical characteristic of a fine white powder. In the course of reaction about 3.6-3.8 ml water was removed from the reaction media and acquired in the Dean Stark apparatus.

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트

후처리

  1. customprovided with a reflux condenser
  2. temperatureThe reaction mixture was cooled
  3. filtrationwas thereafter filtered

출처 및 근거

ORD 기록
ord-3754024031f541969f483a6e6abb888c
출처 데이터셋
uspto-grants-2003_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06670494B1

반응 노트

불러오는 중…