Sodium Iodide → HCID 22411662, 화합물

HRID 439543

반응식

[CH3:1][O:2][C:3]1[C:10]([O:11][CH3:12])=[CH:9][C:6]([CH2:7]O)=[C:5]([N+:13]([O-:15])=[O:14])[CH:4]=1.C(Br)(Br)(Br)Br.C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.COC1C(OC)=CC(CBr)=C([N+]([O-])=O)C=1.[I-:55].[Na+]>>[CH3:1][O:2][C:3]1[C:10]([O:11][CH3:12])=[CH:9][C:6]([CH2:7][I:55])=[C:5]([N+:13]([O-:15])=[O:14])[CH:4]=1

참가 물질

반응물 5

HCID 5238Sodium Iodide

HCID 11205Carbon tetrabromide

HCID 11776Triphenylphosphine

HCID 660976-Nitroveratryl alcohol

HCID 30168121-(Bromomethyl)-2-nitro-4,5-dimethoxybenzene

생성물 1

HCID 22411662HCID 22411662, 화합물

실험 절차

The reaction of 4,5-dimethoxy-2-nitrobenzyl alcohol, carbon tetrabromide and triphenylphosphine is used to generate 4,5-dimethoxy-2-nitrobenzyl bromide, which is then treated with sodium iodide to give 4,5-dimethoxy-2-nitrobenzyl iodide (2).

출처 및 근거

ORD 기록: ord-00984b09d9f447eb86db380bb9d81956
출처 데이터셋: uspto-grants-1996_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05514710

연결된 노트

불러오는 중…