Sulfuric Acid → Benzene, ethenyl-, polymer with 1,3-butadiene

HRID 460400

반응식

HRID 460400 반응식
[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH2:5]=[CH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C([O-])(=O)CCCCCCC/C=C\CCCCCCCC.[K+].O=C[C@@H]([C@H]([C@@H]([C@@H](CO)O)O)O)O.[O-]P(OP([O-])([O-])=O)(=O)[O-].[Na+].[Na+].[Na+].[Na+].S(=O)(=O)(O)O>O>[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH2:5]=[CH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1

참가 물질

8

반응물 6

HCID 1118Sulfuric AcidHCID 7501StyreneHCID 78451,3-ButadieneHCID 24403Tetrasodium PyrophosphateHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanalHCID 23665571Potassium Oleate

생성물 1

HCID 62697Benzene, ethenyl-, polymer with 1,3-butadiene

시약·촉매·용매 1

HCID 962Water용매

실험 절차

50 parts of butadiene rubber latex powder, 50 parts of styrene and 150 parts of deionized water were blended. To the blend, 1.0 parts of potassium oleate, 0.4 parts of cumenhydroperoxide, 0.2 parts of mercaptan-containing chain transfer agent, 0.4 parts of glucose, 0.01 parts of ferrous sulfate hydrate, and 0.3 parts of sodium pyrophosphate were added. The blend was kept at 75° C. for 5 hours to obtain g-ABS latex. To the g-ABS latex, 0.4 parts of sulfuric acid was added, coagulated and dried to obtain butadiene-styrene graft copolymer resin (g-BS) in a powder form.

후처리

  1. additionwere added
  2. customto obtain g-ABS latex
  3. customdried

출처 및 근거

ORD 기록
ord-6c240420062249dfb41ba0ba3e9b74eb
출처 데이터셋
uspto-grants-2007_03
특허 번호
US07196126B2

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