Diazomethane → 3'-Sulfamoyl-diazoacetophenone

HRID 461163

반응식

HRID 461163 반응식
[S:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8](Cl)=[O:9])(=[O:4])(=[O:3])[NH2:2].[N+:14](=[CH2:16])=[N-:15]>C(OCC)C>[S:1]([C:5]1[CH:6]=[C:7]([C:8](=[O:9])[CH:16]=[N+:14]=[N-:15])[CH:11]=[CH:12][CH:13]=1)(=[O:4])(=[O:3])[NH2:2]

참가 물질

4

반응물 2

HCID 9550DiazomethaneHCID 188018833-Sulfamoylbenzoyl chloride

생성물 1

HCID 537058143'-Sulfamoyl-diazoacetophenone

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.

후처리

  1. filtrationthe crystals were filtered off

출처 및 근거

ORD 기록
ord-29a7aeba45ad449fbac66113ff177cd3
출처 데이터셋
uspto-grants-1977_12
특허 번호
US04061761

연결된 노트

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