1,4-Dibromobutane → 1-Bromo-5,8,11-trioxadodecane

반응식

[Na].[CH3:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][OH:9].[Br:10][CH2:11][CH2:12][CH2:13][CH2:14]Br>>[Br:10][CH2:11][CH2:12][CH2:13][CH2:14][O:9][CH2:8][CH2:7][O:6][CH2:5][CH2:4][O:3][CH3:2]

참가 물질

반응물 3

HCID 80561,4-Dibromobutane

HCID 8134Diethylene Glycol Monomethyl Ether

HCID 5360545Sodium

생성물 1

HCID 234315621-Bromo-5,8,11-trioxadodecane

실험 절차

This compound is prepared in a way similar to that in paragraph 1/ of example 1) by reacting the sodium salt of diethylene glycol monomethyl ether with an excess of 1,4-dibromobutane. Column purification gives a yellow-colored oil.

후처리

customThis compound is prepared in a way similar to that in paragraph 1/ of example 1)
customColumn purification
customgives a yellow-colored oil

출처 및 근거

ORD 기록: ord-cbb03d11116b46d485de275a631d6839
출처 데이터셋: uspto-grants-2004_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06699954B2

반응 노트

불러오는 중…