Ammonia → Quinacridone

HRID 479899

반응식

HRID 479899 반응식
C[C:2]1[CH:7]=[CH:6][C:5]2[NH:8][C:9]3[C:14]([C:15](=[O:16])[C:4]=2[CH:3]=1)=[CH:13][C:12]1[NH:17][C:18]2[CH:25]=[CH:24][C:23](C)=[CH:22][C:19]=2[C:20](=[O:21])[C:11]=1[CH:10]=3.CC1C=CC(S(NC2C=C(S([O-])(=O)=O)C=C3C=C(S([O-])(=O)=O)/C(/C(=O)C=23)=N/NC2C=C(Cl)C=CC=2OC2C=CC=CC=2)(=O)=O)=CC=1.[Na+].[Na+].N>O>[CH:23]1[CH:22]=[C:19]2[C:20]([C:11]3[C:12]([NH:17][C:18]2=[CH:25][CH:24]=1)=[CH:13][C:14]1[C:15]([C:4]2[C:5]([NH:8][C:9]=1[CH:10]=3)=[CH:6][CH:7]=[CH:2][CH:3]=2)=[O:16])=[O:21]

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 704235,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dioneHCID 178427422HCID 178427422, 화합물

생성물 1

HCID 13976Quinacridone

시약·촉매·용매 1

HCID 962Water용매5회

실험 절차

20 g of C.I. pigment red 122 having an average primary particle diameter of 90 nm (in which the content of metal ions having a valence of at least 2 was 450 ppm), 4 g of a commercially available dye C.I. acid red 249 and 110 g of deionized water were mixed, aqueous ammonia was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion had a high viscosity and caused flocculation. Further, the water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped on No.2 filter paper, to show bleeding of the dye.

후처리

  1. additionwas diluted so as
  2. additionwas dropped on No.2 filter paper

출처 및 근거

ORD 기록
ord-a93018f0c5a346c381a6a0cd5b462802
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06648954B2

연결된 노트

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