Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)

HRID 480987

반응식

HRID 480987 반응식
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[C:9](#[N:12])[CH:10]=[CH2:11].CC(N=NC(C#N)(C)C)(C#N)C.P([O-])([O-])([O-])=O.[Ca+2].[Ca+2].[Ca+2].P([O-])([O-])([O-])=O>O>[CH2:11]=[CH:10][C:9]#[N:12].[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

6

반응물 4

HCID 6547AzobisisobutyronitrileHCID 7501StyreneHCID 7855AcrylonitrileHCID 24456Tricalcium Phosphate

생성물 1

HCID 62696Prop-2-enenitrile--ethenylbenzene (1/1)

시약·촉매·용매 1

HCID 962Water용매

실험 절차

75 parts of styrene, 25 parts of acrylonitrile, 120 parts of deionized water and 0.2 parts of azobisisobutylonitrile were blended. To the blend, 0.4 parts of tricalciumphosphate and 0.2 parts of mercaptan-containing chain transfer agent were added. The resultant solution was heated to 80° C. for 90 minutes and kept for 180 minutes. The resultant was washed, dehydrated and dried to produce SAN powder. styrene-acrylonitrile copolymer (SAN) having a weight average molecular weight of 160,000 to 200,000 was obtained.

후처리

  1. additionwere added
  2. washThe resultant was washed
  3. customdried

출처 및 근거

ORD 기록
ord-7a0b5fcd64b04b578922b657f61465d0
출처 데이터셋
uspto-grants-2003_11
특허 번호
US06653374B1

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