홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Formaldehyde → Melamine formaldehyde

HRID 484923
노트
인쇄 미리보기

반응식

HRID 484923 반응식
C(OCCCCCCCCCCCC)(=O)C1C=C(O)C(O)=[C:4]([OH:5])C=1.C(OCCC(C)C)(=O)C1C=C(O)C(O)=C(O)C=1.[OH-].[Na+].[N:44]1[C:51]([NH2:52])=[N:50][C:48]([NH2:49])=[N:47][C:45]=1[NH2:46].C=O>C(OCC)(=O)CCCCC(OCC)=O.C(O)CCCCCCC/C=C\CCCCCCCC.O>[CH2:4]=[O:5].[N:44]1[C:51]([NH2:52])=[N:50][C:48]([NH2:49])=[N:47][C:45]=1[NH2:46]
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

9

반응물 5

HCID 712FormaldehydeHCID 7955MelamineHCID 14425Dodecyl GallateHCID 14798Sodium Hydroxide2회HCID 75596Isoamyl gallate

생성물 1

HCID 93374Melamine formaldehyde

시약·촉매·용매 3

HCID 962
Water
용매
HCID 8844Diethyl Adipate용매
HCID 5284499Oleyl Alcohol용매

반응 조건

온도
80 °C

실험 절차

A 15 part quantity of lauryl gallate and 5 parts of isoamyl gallate were dissolved in a mixture of 70 parts of diethyl adipate and 30 parts of oleyl alcohol with heating to prepare an oil. The oil was added to 100 parts of 5% aqueous solution having a pH of 5 and containing SCRIPSET 520 (trade name of styrene-maleic anhydride copolymer, product of Monsant Co.) and a small amount of sodium hydroxide, and emulsified to obtain a dispersion of particles 4.0μ in average size. Ten parts of melamine and 25 parts of 37% aqueous solution of formaldehyde were added to 65 parts of water. The mixture was adjusted to a pH of 9 with sodium hydroxide and heated to 80° C. for 15 minutes, whereby a melamine-formaldehyde initial condensate was obtained. The dispersion was added to the condensate and the mixture was stirred for 1 hour at 75° C. to prepare a microcapsule dispersion.

후처리

  1. temperaturewith heating
  2. customto prepare an oil
  3. customto obtain a dispersion of particles 4.0μ in average size

출처 및 근거

ORD 기록
ord-c1af9ba64f7f4e8f90ce854a4b302c7a
출처 데이터셋
uspto-grants-1985_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04533930

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트