Azobisisobutyronitrile → Methyl 3-(bromomethyl)benzoate

HRID 4912

반응식

HRID 4912 반응식
[C:1]1([CH3:11])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]([O:9][CH3:10])=[O:8])[CH:2]=1.C1C(=O)N([Br:19])C(=O)C1.CC(N=NC(C#N)(C)C)(C#N)C>>[Br:19][CH2:11][C:1]1[CH:2]=[C:3]([CH:4]=[CH:5][CH:6]=1)[C:7]([O:9][CH3:10])=[O:8]

참가 물질

4

실험 절차

Methyl m-toluate was brominated with NBS and AIBN as described in Example 21 to give methyl m-bromomethylbenzoate, and this was further reacted with triethyl phosphite as described in Example 2 without further purification.

출처 및 근거

ORD 기록
ord-72cd4b260c0043e8aa2503a92dce1f5e
출처 데이터셋
uspto-grants-1993_09
특허 번호
US05242908

연결된 노트

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