반응식
[H-].[Na+].[CH:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][C:4]=1[O:13][CH2:14][CH2:15][OH:16].[Cl:17][C:18]1[C:23](Cl)=[N:22][CH:21]=[CH:20][N:19]=1>O1CCOCC1>[Cl:17][C:18]1[C:23]([O:16][CH2:15][CH2:14][O:13][C:4]2[CH:5]=[CH:6][C:7]3[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:3]=2)=[N:22][CH:21]=[CH:20][N:19]=1참가 물질
5
반응 조건
- 온도
- 40 °C
실험 절차
Sodium hydride (55% dispersion in mineral oil; 44 mg, 1.0 mmol) was added to a mixture of 2-(2-naphthoxy)ethanol (188 mg, 1.00 mmol) and 2,3-dichloropyrazine (149 mg, 1.00 mmol) in dioxane (0.5 mL), and the reaction mixture was stirred at 40° C. for 15 h. The crude material was used directly in Step 2.
출처 및 근거
- ORD 기록
- ord-bfed6779a35d4e33a019655fe10f3cc9
- 출처 데이터셋
- uspto-grants-2009_05
- 특허 번호
- US07534794B2
연결된 노트
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