Triethoxysilane → Triethoxy(3-isocyanatopropyl)silane

HRID 52685

반응식

HRID 52685 반응식
[CH2:1]([N:4]=[C:5]=[O:6])[CH:2]=[CH2:3].[CH2:7]([O:9][SiH:10]([O:14][CH2:15][CH3:16])[O:11][CH2:12][CH3:13])[CH3:8]>CC1C=CC(C)=CC=1>[N:4]([CH2:1][CH2:2][CH2:3][Si:10]([O:14][CH2:15][CH3:16])([O:11][CH2:12][CH3:13])[O:9][CH2:7][CH3:8])=[C:5]=[O:6]

참가 물질

4

반응물 2

HCID 13830TriethoxysilaneHCID 15123Allyl isocyanate

생성물 1

HCID 90613Triethoxy(3-isocyanatopropyl)silane수율 71.8%

시약·촉매·용매 1

HCID 7809P-Xylene용매

실험 절차

In analogy to Example 6, a reaction mixture consisting of 640 g of p-xylene, 680 g (8.17 mol) of allyl isocyanate and 1250 g (7.6 mol) of triethoxysilane was reacted at from 76° to 92° C. over the course of 150 minutes. Working up by distillation gave 1350 g of 3-isocyanatopropyltriethoxysilane in addition to the trimer.

후처리

  1. customwas reacted at from 76° to 92° C. over the course of 150 minutes
  2. distillationWorking up by distillation

출처 및 근거

ORD 기록
ord-a6b7d28bd66448d9ab588797d7716d9f
출처 데이터셋
uspto-grants-1997_04
특허 번호
US05616762

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