Hydrochloric Acid → HCID 131713514, 화합물

HRID 544545

반응식

HRID 544545 반응식
[Cl-].[Na+].[CH3:3][P:4]([CH2:6][CH2:7][P:8]([CH3:10])[CH3:9])[CH3:5].Cl.[CH2:12]([OH:14])[CH3:13]>>[CH2:12]([OH:14])[CH3:13].[CH3:3][P:4]([CH2:6][CH2:7][P:8]([CH3:10])[CH3:9])[CH3:5]

참가 물질

5

반응물 4

HCID 313Hydrochloric AcidHCID 702Ethanol2회HCID 5234Sodium Chloride2회HCID 1410591,2-Bis(dimethylphosphino)ethane

생성물 1

HCID 131713514HCID 131713514, 화합물수율 80%

실험 절차

Prepare a saturated solution of sodium chloride in ethanol by dissolving 117 mg of sodium chloride in 20 ml of degassed ethanol. Add 11.1 μl of liquid DMPE to this solution and adjust its pH to approximately 2.25 by adding concentrated hydrochloric acid. Dispense 5 ml into a 10 cc vial and crimp seal it using a teflon-coated stopper. Inject approximately 5 mCi of 99mTc-pertechnetate eluate into the vial and place it in a boiling water bath for 1 hour. HPLC analysis shows a yield of greater than 80% of the [99mTcCl2 (DMPE)2 ]+ complex.

후처리

  1. customDispense 5 ml into a 10 cc vial and crimp seal it

출처 및 근거

ORD 기록
ord-9a0dc57b1aae4ff8b16c6303cf18cc6d
출처 데이터셋
uspto-grants-1984_05
특허 번호
US04451450

연결된 노트

불러오는 중…