Hydrazine hydrate (1:1) → HCID 21327244, 화합물

HRID 614843노트

반응식

HRID 614843 반응식
[CH2:1]([O:8][C:9]1[CH:14]=[C:13]([C:15]([CH3:18])([CH3:17])[CH3:16])[CH:12]=[C:11]([N+:19]([O-])=O)[C:10]=1[CH3:22])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.O.NN>[Ni].CO>[CH2:1]([O:8][C:9]1[CH:14]=[C:13]([C:15]([CH3:16])([CH3:17])[CH3:18])[CH:12]=[C:11]([NH2:19])[C:10]=1[CH3:22])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

5

반응물 2

HCID 24654Hydrazine hydrate (1:1)HCID 213273062-Methyl-3-nitro-5-tert.-butylphenyl benzyl ether

생성물 1

HCID 21327244HCID 21327244, 화합물

시약·촉매·용매 2

HCID 935Nickel촉매HCID 887Methanol용매

실험 절차

This is obtained, by reducing 2-methyl-3-nitro-5-tert.-butylphenyl benzyl ether with hydrazine hydrate and Raney nickel in methanol, in the form of a pale brown oil.

후처리

  1. customThis is obtained

출처 및 근거

ORD 기록
ord-b3e86c481ec8402290bb0774f8d1e6c1
출처 데이터셋
uspto-grants-1979_03
특허 번호
US04146630

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