Ethylene Glycol → 1-(3-Pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide
반응식
[BrH:1].[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][NH:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-:21])=[O:20])=[CH:15][CH:14]=2)=[O:11])[CH:3]=1.C(O)CO.CCOCC>COC>[BrH:1].[N:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][NH:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-:21])=[O:20])=[CH:15][CH:14]=2)=[O:11])[CH:3]=1참가 물질
6
실험 절차
Gaseous HBr was passed into a solution of 3 g. of 3-pyridylmethyl-3-(4-nitrophenyl)urea in the monomethyl ether of ethyleneglycol. Ether was added to give a precipitate and after isolation, washing with ether and drying, 2.95 g. of white solid was obtained. This was a 76% yield of 1-(3-pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide.
후처리
- customto give a precipitate
- washafter isolation, washing with ether
- customdrying
- customof white solid was obtained
출처 및 근거
- ORD 기록
- ord-8516dea8be604bd1a9ad11bb6a843748
- 출처 데이터셋
- uspto-grants-1978_02
- 특허 번호
- US04075345
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