Dimethyladipate → Disodium adipate

HRID 65824

반응식

HRID 65824 반응식
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].[OH-].[Na+:14]>C(#N)C>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:14].[Na+:14]

참가 물질

4

반응물 2

HCID 12329DimethyladipateHCID 14798Sodium Hydroxide

생성물 1

HCID 24073Disodium adipate

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

후처리

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution was filtered hot
  3. customdried

출처 및 근거

ORD 기록
ord-af3c1eef92454c249d5f397014b710cf
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04129520

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