Diazomethane → Methyl 3,5-Dibromobenzoate

HRID 658247

반응식

HRID 658247 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([OH:7])=[O:6].[N+](=[CH2:14])=[N-]>CCOCC>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([O:7][CH3:14])=[O:6]

참가 물질

4

반응물 2

HCID 9550DiazomethaneHCID 12063Benzoic acid, 3,5-dibromo-

생성물 1

HCID 621923Methyl 3,5-Dibromobenzoate

시약·촉매·용매 1

HCID 3283Diethyl Ether용매2회

실험 절차

To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.

후처리

  1. concentrationconcentrated in vacuo

출처 및 근거

ORD 기록
ord-c9c0b78b58ea4da49f17993ef5b5aaae
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08076359B2

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