Diazomethane → Methyl 3,5-Dibromobenzoate
반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([OH:7])=[O:6].[N+](=[CH2:14])=[N-]>CCOCC>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([Br:11])[CH:10]=1)[C:5]([O:7][CH3:14])=[O:6]참가 물질
4
실험 절차
To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.
후처리
- concentrationconcentrated in vacuo
출처 및 근거
- ORD 기록
- ord-c9c0b78b58ea4da49f17993ef5b5aaae
- 출처 데이터셋
- uspto-grants-2011_12
- 특허 번호
- US08076359B2
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