Hydrochloric Acid → 2-Acetylthio-3-methoxybenzoic acid

HRID 67900노트

반응식

HRID 67900 반응식
[SH:1][C:2]1[C:10]([O:11][CH3:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[C:13](OC(=O)C)(=[O:15])[CH3:14].Cl>C(O)(=O)C>[C:13]([S:1][C:2]1[C:10]([O:11][CH3:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:15])[CH3:14]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 7918Acetic AnhydrideHCID 166556102-Mercapto-3-methoxybenzoic acid

생성물 1

HCID 204652112-Acetylthio-3-methoxybenzoic acid

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

A solution of 2-mercapto-3-methoxybenzoic acid (14.6 g, 79 mmol), acetic anhydride (9.7 g, 95 mmol) and glacial acetic acid (35 ml) was refluxed 15 minutes, then cooled and poured into dilute hydrochloric acid.

후처리

  1. temperaturecooled

출처 및 근거

ORD 기록
ord-bca570220ba24229a752eb77e5c21fd5
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04347246

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