Styrene → 1,1-Diphenylethylene

HRID 68032

반응식

HRID 68032 반응식
C=Cc1ccccc1.O=S(=O)(Oc1ccccc1)C(F)(F)F>CC(C)(C)P1CN(c2ccc(C(F)(F)F)cc2)CP(C(C)(C)C)CN(c2ccc(C(F)(F)F)cc2)C1.CCN(CC)CC.Cc1ccccc1.C1=C\CC/C=C\CC/1.C1=C\CC/C=C\CC/1.[Ni]>C=C(c1ccccc1)c1ccccc1.COc1cc(OC)cc(OC)c1.C(=C\c1ccccc1)/c1ccccc1

참가 물질

9

반응물 2

HCID 7501StyreneHCID 548641Phenyl Trifluoromethanesulfonate

생성물 3

HCID 107401,1-DiphenylethyleneHCID 693011,3,5-TrimethoxybenzeneHCID 638088trans-Stilbene

시약·촉매·용매 4

HCID 8471Triethylamine시약HCID 1778483303,7-Di-tert-butyl-1,5-bis(4-(trifluoromethyl)phenyl)-1,5,3,7-diazadiphosphocane촉매HCID 1140Toluene용매HCID 6433264Bis(1,5-cyclooctadiene)nickel기타

반응 조건

온도
85 °C

후처리

  1. additionFiltrate 상 유지

출처 및 근거

ORD 기록
ord-c81bab83314a47db87e8b8809ef91417
출처 데이터셋
Styrene Mizoroki-Heck

연결된 노트

불러오는 중…