Diethyl Ether → HCID 22597223, 화합물

HRID 7193

반응식

HRID 7193 반응식
[CH3:1][C:2]1(O)[CH:9]2[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:11][CH:3]1[CH2:4]3)[CH2:8]2.[C:13](Cl)(=[O:16])[CH:14]=[CH2:15].C([O:20]CC)C>>[C:13]([O:16][C:3]12[CH2:11][CH:7]3[CH2:6][CH:5]([CH2:10][CH:9]([CH2:8]3)[CH:2]1[CH3:1])[CH2:4]2)(=[O:20])[CH:14]=[CH2:15]

참가 물질

4

반응물 3

HCID 3283Diethyl EtherHCID 13140Acryloyl chlorideHCID 1365452-Methyl-2-adamantanol

생성물 1

HCID 22597223HCID 22597223, 화합물수율 55%

실험 절차

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

후처리

  1. customThe reactant was reacted at room temperature for about 12 hours
  2. filtrationfiltered
  3. customSubsequently, the solvent was removed by an evaporator
  4. customthe reactant product was obtained
  5. distillationvacuum distillation (yield: 55%)

출처 및 근거

ORD 기록
ord-36f2de1457284bf3b0fda06e472eab7b
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07084227B2

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