Hydrochloric Acid → Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride

HRID 747666

반응식

HRID 747666 반응식
[C:1]([C:3]1[CH:13]=[CH:12][C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[CH:5][CH:4]=1)#[N:2].[ClH:14].[CH2:15]([OH:17])[CH3:16]>O1CCOCC1>[ClH:14].[CH2:15]([O:17][C:1]([C:3]1[CH:13]=[CH:12][C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[CH:5][CH:4]=1)=[NH:2])[CH3:16]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 81589Ethyl 4-cyanobenzoate

생성물 1

HCID 68830640Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

5.16 g (29 mmol) of ethyl 4-cyanobenzoate was stirred in 50 ml of 4N solution of hydrogen chloride in dioxane. 5 ml of ethanol was added to the resultant mixture, and they were stirred at room temperature for 4 days. The solvent was evaporated, and the residue was washed with ethyl acetate and dried to obtain the title compound.

후처리

  1. customThe solvent was evaporated
  2. washthe residue was washed with ethyl acetate
  3. customdried

출처 및 근거

ORD 기록
ord-745c474fe6424adb93f48ea986009b47
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07396844B1

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