3,5-Dimethylbenzoic acid → N-methoxy-N,3,5-trimethylbenzamide

반응식

CNOC.Cc1cc(C)cc(C(=O)O)c1.CN(C)C(=[N+](C)C)F.F[P-](F)(F)(F)(F)F.CN(C)C1=CC=NC=C1.CCN(C(C)C)C(C)C.CN(C)C=O>>CON(C)C(=O)c1cc(C)cc(C)c1

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

불러오는 중…

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

불러오는 중…