4-Hydroxybenzoic Acid → Benzoic acid, 4-((1-oxodecyl)oxy)-

HRID 752

반응식

HRID 752 반응식
[OH:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[C:11](Cl)(=[O:21])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].N1C=CC=CC=1>O>[C:11]([O:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1)(=[O:21])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

참가 물질

5

반응물 3

HCID 1354-Hydroxybenzoic AcidHCID 1049PyridineHCID 66982Decanoyl chloride

생성물 1

HCID 3608562Benzoic acid, 4-((1-oxodecyl)oxy)-

시약·촉매·용매 1

HCID 962Water용매

실험 절차

10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.

후처리

  1. extractionan organic layer was extracted with dichloromethane
  2. washThe organic layer was washed with 1N hydrochloric acid
  3. dry with materialdried over anhydrous sodium sulfate
  4. distillationthe solvent was distilled off
  5. washresidue was washed with n-hexane
  6. customdried
  7. customto give a crude end product

출처 및 근거

ORD 기록
ord-c218088b16c541088a933a7606f68c4c
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05723069

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