N-Methyl-4-anisidine → HCID 178492277, 화합물
반응식
CNc1ccc(OC)cc1.Cc1c(C(=O)O)oc2ccccc12.C1CCC(CC1)N=C=NC2CCCCC2.C1=C(C(=CC(=C1Cl)Cl)Cl)[O-].[Na+].CN1CCOCC1.CN(C)C=O>>COc1ccc(N(C)C(=O)c2oc3ccccc3c2C)cc1참가 물질
7
반응 조건
- 온도
- 25 °C
후처리
- addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
- aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
- addition380 uL MeCN solvent were added to the transfer plate
- aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
- addition180 uL MeCN added to filter plate 1 for LCMS analysis
- aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
- addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
- customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM
출처 및 근거
- ORD 기록
- ord-607afe4bc6e94c41b1545b6a25a79d82
- 출처 데이터셋
- AIChemEco amide coupling conditions 47k dataset
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