Hydrogen Peroxide → Peroxide, bis(2-methyl-1-oxopropyl)

HRID 8140

반응식

HRID 8140 반응식
[OH:1][OH:2].[C:3](Cl)(=[O:7])[CH:4]([CH3:6])[CH3:5]>O>[C:3]([O:1][O:2][C:3](=[O:7])[CH:4]([CH3:6])[CH3:5])(=[O:7])[CH:4]([CH3:6])[CH3:5]

참가 물질

4

반응물 2

HCID 784Hydrogen PeroxideHCID 62325Isobutyryl chloride

생성물 1

HCID 76969Peroxide, bis(2-methyl-1-oxopropyl)

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

In Example A, the procedure of WO 01/32613 was repeated. First, a solution of Na2O2 was prepared by combining 108.3 g of demineralized water, 18.5 g of NaOH-33 solution, and 3.7 g of the aqueous H2O2. A second reactor was charged with 33.3 g of demineralized water, 27.7 g of the PVA solution, and 16.3 g of isobutanoyl chloride while controlling the temperature between 5–10° C. Next, the Na2O2 solution was dosed while the system was homogenized. No diisobutanoyl peroxide was obtained and only an aqueous phase formed.

후처리

  1. customFirst, a solution of Na2O2 was prepared
  2. custombetween 5–10° C

출처 및 근거

ORD 기록
ord-9ab80e1ebfc347c382d0c4a31e189f35
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07087693B2

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