Hydrochloric Acid → HCID 15406934, 화합물
반응식
[CH3:1][C:2]([C:9]1[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=1)([CH3:8])[C:3]([O:5]CC)=[O:4].[Li+].[OH-].O.Cl>CCO>[CH3:8][C:2]([C:9]1[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=1)([CH3:1])[C:3]([OH:5])=[O:4]참가 물질
6
반응 조건
- 온도
- 25 °C
실험 절차
Ethyl α,α-dimethyl-3-pyridylacetate (disclosed in EP application 0 288 279, published Oct. 26, 1988) (2.67 grams, 13.8 mmoles) was dissolved in EtOH (11.1 ml.) and a 1.0M LiOH in water (33.3 ml.) (33.4 mmoles) was added. The mixture was stirred at 25° C. for 4 hours. 1 N HCl (38.73 ml.) was added and after 5 minutes the mixture was evaporated to dryness to give the title compound (Yield: 100%).
후처리
- customwas evaporated to dryness
출처 및 근거
- ORD 기록
- ord-276d83f8d5c246c888e8357864494c2c
- 출처 데이터셋
- uspto-grants-2002_04
- 특허 번호
- US06365588B1
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