Acetic Anhydride → HCID 15023231, 화합물

반응식

[NH2:1][CH2:2][CH:3]1[C:12]2[C:7](=[CH:8][C:9]([O:13][CH3:14])=[CH:10][CH:11]=2)[O:6][CH2:5][CH2:4]1.[CH2:15](OC=O)[CH3:16].C(OC(=O)C)(=O)C>>[CH2:15]([NH:1][CH2:2][CH:3]1[C:12]2[C:7](=[CH:8][C:9]([O:13][CH3:14])=[CH:10][CH:11]=2)[O:6][CH2:5][CH2:4]1)[CH3:16]

참가 물질

반응물 3

HCID 7918Acetic Anhydride

HCID 8025Ethyl formate

HCID 15023228HCID 15023228, 화합물

생성물 1

HCID 15023231HCID 15023231, 화합물

실험 절차

The product from Example 2 was reacted as described in Example 3 replacing ethylformate with acetic anhydride, giving the desired product, (M+H)+ 222. 1H NMR(CDCl3): 1.15 (t,3H); 2.05 (m,2H); 2.6-2.0 (m,4H); 3.75 (s,3H); 4.2 (m,1H), 6.3-7.1 (m,3H).

출처 및 근거

ORD 기록: ord-0c36a50ad9ac4796a1c6916412123f4b
출처 데이터셋: uspto-grants-1992_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05140039

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