Hydrochloric Acid → N-(Cyclohexyl)-N-(2-chloroethyl)-aminomethylphosphonic Acid

HRID 848691노트

반응식

HRID 848691 반응식
Cl.[Cl:2][CH2:3][CH2:4][NH:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1.[P:12]([OH:15])([OH:14])[OH:13].Cl.[CH2:17]=O>O>[CH:6]1([N:5]([CH2:17][P:12](=[O:15])([OH:14])[OH:13])[CH2:4][CH2:3][Cl:2])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 107909Phosphorous acidHCID 13756691N-(2-chloroethyl)cyclohexanamine hydrochloride

생성물 1

HCID 20564015N-(Cyclohexyl)-N-(2-chloroethyl)-aminomethylphosphonic Acid

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A total of 101 parts of N-(2-chloroethyl)cyclohexylamine hydrochloride, 41.5 parts phosphorous acid in 101 parts water, 75 parts of 37% aqueous hydrochloric acid, and 104 parts of 37% aqueous formaldehyde were used to prepare Reagent E-2.

후처리

  1. customto prepare Reagent E-2

출처 및 근거

ORD 기록
ord-5b2219caef99433fa30a1df3d6e54b03
출처 데이터셋
uspto-grants-1981_10
특허 번호
US04297299

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