Hydrochloric Acid → HCID 178479039, 화합물

HRID 849081

반응식

HRID 849081 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:3]=1.[ClH:15]>[Pt]=O>[ClH:15].[CH:9]1([CH2:8][CH:4]2[NH:3][C:2](=[NH:1])[CH2:7][CH2:6][CH2:5]2)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 939026-Benzylpyridin-2-amine

생성물 1

HCID 178479039HCID 178479039, 화합물

시약·촉매·용매 1

HCID 82844Platinum oxide (PtO)촉매

실험 절차

The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.

후처리

  1. customThe product was obtained as an oil which
  2. customto give a white solid
  3. customThe solid was recrystallized from EtOAc

출처 및 근거

ORD 기록
ord-ab961bebbe72482badb3276f57ec740a
출처 데이터셋
uspto-grants-2000_01
특허 번호
US06011028

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