Sodium Hydroxide → Leucinamide

HRID 864277

반응식

HRID 864277 반응식
[NH2:1][C@H:2]([C:7]([NH2:9])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5].Cl.[OH-].[Na+]>CC(N(C)C)=O.O>[NH2:1][C@H:2]([C:7]([NH2:9])=[O:8])[CH2:3][CH:4]([CH3:6])[CH3:5]

참가 물질

5

반응물 2

HCID 14798Sodium HydroxideHCID 2733199Leucinamide hydrochloride

생성물 1

HCID 69640Leucinamide

시약·촉매·용매 2

HCID 962Water용매HCID 31374Dimethylacetamide용매2회

실험 절차

1.25M solution of Leu-NH2 in DMAC was prepared by dissolving Leu-NH2.HCl (1.33 g, 7.98 mmol) in 5.0 mL of water, titrating to pH 8.0 with 1M NaOH, lyophilizing, and taking up the residue in 6.4 ml of DMAC. The NaCl precipitate was removed by filtering through a fine glass frit to give a clear solution of pH 9.25.

후처리

  1. customThe NaCl precipitate was removed
  2. filtrationby filtering through a fine glass frit
  3. customto give a clear solution of pH 9.25

출처 및 근거

ORD 기록
ord-b5d127ef1e6044608b68a102b37d5fbf
출처 데이터셋
uspto-grants-1996_10
특허 번호
US05563044

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