Acetic Acid → HCID 75985013, 화합물
반응식
Br[CH2:2][C:3]([O:11][CH3:12])=[CH:4][C:5](=[O:10])[C:6]([Cl:9])([Cl:8])[Cl:7].[C:13]([O-:16])(=[O:15])[CH3:14].[K+].C(O)(=O)C>[Br-].C([N+](CCCC)(CCCC)CCCC)CCC.C(#N)C>[C:13]([O:16][CH2:2][C:3]([O:11][CH3:12])=[CH:4][C:5](=[O:10])[C:6]([Cl:9])([Cl:8])[Cl:7])(=[O:15])[CH3:14]참가 물질
6
실험 절차
29.6 g (0.1 mol) of 5-bromo-1,1,1-trichloro-4-methoxypent-3-en-2-one, 17 g of potassium acetate, 5 g of tetrabutylammonium bromide and 8 g of acetic acid were stirred in 300 ml of acetonitrile at 40° C. for 16 h. The mixture was concentrated under reduced pressure, and water was added to the residue. The product was extracted with ethyl acetate, the organic phase was washed with water and the solvent was removed fully under reduced pressure.
후처리
- concentrationThe mixture was concentrated under reduced pressure, and water
- additionwas added to the residue
- extractionThe product was extracted with ethyl acetate
- washthe organic phase was washed with water
- customthe solvent was removed fully under reduced pressure
출처 및 근거
- ORD 기록
- ord-6997653a992545bf94ed3d2618fd6555
- 출처 데이터셋
- uspto-grants-2012_08
- 특허 번호
- US08242313B2
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