Azobisisobutyronitrile → 3-(Bromomethyl)biphenyl

HRID 893368

반응식

HRID 893368 반응식
[C:1]1([C:7]2[CH:8]=[C:9]([CH3:13])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Br:14]N1C(=O)CCC1=O.N(C(C)(C)C#N)=NC(C)(C)C#N>C(Cl)(Cl)(Cl)Cl>[C:1]1([C:7]2[CH:8]=[C:9]([CH:10]=[CH:11][CH:12]=2)[CH2:13][Br:14])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

5

반응물 3

HCID 6547AzobisisobutyronitrileHCID 125643-MethylbiphenylHCID 67184N-bromobutanimide

생성물 1

HCID 38644053-(Bromomethyl)biphenyl

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매

실험 절차

3-Phenylbenzyl bromide (melting point 54°-56° C.) was prepared by illumination of a solution of 3-phenyltoluene and N-bromosuccinimide in carbon tetrachloride in the presence of azobisisobutyronitrile.

출처 및 근거

ORD 기록
ord-84753b0b196246baa90020c475bce886
출처 데이터셋
uspto-grants-1992_06
특허 번호
US05124353

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