Fluorine → Acrylic acid ethyl acrylate

HRID 914650노트

반응식

HRID 914650 반응식
[Na].[C:2]([C:10]([O:16][CH2:17][CH2:18][O:19][C:20]1C=CC=[CH:22][CH:21]=1)(S([O-])(=O)=O)C)(CC(C)(C)C)(C)[CH3:3].[Na+].S1(=[O:36])C2C=CC=CC=2C=N1.FF.[K]>>[C:20]([OH:36])(=[O:19])[CH:21]=[CH2:22].[C:10]([O:16][CH2:17][CH3:18])(=[O:36])[CH:2]=[CH2:3]

참가 물질

6

반응물 5

HCID 24524Fluorine6회HCID 5360545SodiumHCID 5462222PotassiumHCID 159622201H-1lambda~4~,2-Benzothiazol-1-oneHCID 86589510Sodium t-octylphenoxyethoxyethanesulfonate

생성물 1

HCID 168277Acrylic acid ethyl acrylate수율 51,513.801%

실험 절차

A coating solution for protective layer on the back side was prepared by mixing 50 g of gelatin, 0.2 g of sodium polystyrenesulfonate, 2.4 g of N,N-ethylenebis(vinylsulfonacetamide), 1 g of sodium tert-octylphenoxyethoxyethanesulfonate, 30 mg of benzisothiazolinone, 37 mg of a fluorine-containing surfactant (F-1: potassium salt of N-perfluorooctylsulfonyl-N-propylalanine), 150 mg of a fluorine-containing surfactant (F-2: polyethylene glycol mono(N-perfluorooctylsulfonyl-N-propyl-2-aminoethyl) ether [average polymerization degree of ethylene oxide: 15]), 64 mg of a fluorine-containing surfactant (F-3), 32 mg of a fluorine-containing surfactant (F-4), 10 mg of a fluorine-containing surfactant (F-7), 5 mg of a fluorine-containing surfactant (F-8), 8.8 g of acrylic acid/ethyl acrylate copolymer (copolymerization ratio: 5/95 by weight), 0.6 g of Aerosol-OT (produced by American Cyanamid Co.), a liquid paraffin emulsion containing 1.8 g of liquid paraffin and 950 ml of water in a vessel kept at 40° C.

후처리

  1. customA coating solution for protective layer on the back side was prepared
  2. additioncontaining

출처 및 근거

ORD 기록
ord-6dfdb4ffa6624d25b5b5f1e73b8e686c
출처 데이터셋
uspto-grants-2007_09
특허 번호
US07264919B2

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