Glycine → N-(1-Oxodecyl)glycine

HRID 979748노트

반응식

HRID 979748 반응식
[C:1]([Cl:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[NH2:13][CH2:14][C:15]([OH:17])=[O:16]>>[C:1]([Cl:12])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[NH2:13][CH2:14][C:15]([OH:17])=[O:16].[C:1]([NH:13][CH2:14][C:15]([OH:17])=[O:16])(=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

참가 물질

5

반응물 2

HCID 750GlycineHCID 66982Decanoyl chloride

생성물 3

HCID 750GlycineHCID 66982Decanoyl chlorideHCID 1712391N-(1-Oxodecyl)glycine수율 94%

실험 절차

N-Decanoylglycine was prepared by reaction of decanoyl chloride with glycine according to the procedure described in Example I. From 47.7 g (0.25 mol) of decanoyl chloride and 18.8 g (0.25 mol) of glycine was obtained 54.1 g (94%) of N-decanoylglycine, mp 104°-108° C.

출처 및 근거

ORD 기록
ord-0eb27852a82d4d72adeebc6964bdc46c
출처 데이터셋
uspto-grants-1987_01
특허 번호
US04634551

반응 노트

불러오는 중…