Hydroxyacetonitrile → (Dodecylamino)acetonitrile

HRID 980862

반응식

HRID 980862 반응식
O[CH2:2][C:3]#[N:4].[CH2:5]([NH2:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CO>[CH2:5]([NH:17][CH2:2][C:3]#[N:4])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

참가 물질

4

반응물 2

HCID 7857HydroxyacetonitrileHCID 13583Dodecylamine

생성물 1

HCID 222308(Dodecylamino)acetonitrile

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

In a flask of 500 ml provided with a magnetic stirrer, 4.56 gr of hydroxyacetonitrile (0.08 mol) were mixed at room temperature with 16.3 gr of dodecylamine (0.088 mol) in 250 ml of methanol. The mixture was allowed to stand for 16 hours at room temperature and methanol was evaporated. The obtained liquid was distilled under 10-2 mm Hg. The fraction distilling between 106° and 116° crystallizes after cooling.

후처리

  1. customIn a flask of 500 ml provided with a magnetic stirrer
  2. custommethanol was evaporated
  3. distillationThe obtained liquid was distilled under 10-2 mm Hg
  4. distillationThe fraction distilling between 106° and 116°
  5. customcrystallizes
  6. temperatureafter cooling

출처 및 근거

ORD 기록
ord-062b5b872d41428695569fdb5abf608a
출처 데이터셋
uspto-grants-1987_01
특허 번호
US04639468

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