Hydrochloric Acid → Iminoethyl methoxyacetate hydrochloride

HRID 992650

반응식

HRID 992650 반응식
[CH3:1][O:2][CH2:3][C:4]#[N:5].C([OH:8])C.[ClH:9].[CH2:10]([O:12][CH2:13]C)C>>[ClH:9].[CH3:10][O:12][CH2:13][C:1]([O:2][CH2:3][CH:4]=[NH:5])=[O:8]

참가 물질

5

반응물 4

HCID 313Hydrochloric AcidHCID 702EthanolHCID 3283Diethyl EtherHCID 74442Methoxyacetonitrile

생성물 1

HCID 57478929Iminoethyl methoxyacetate hydrochloride

실험 절차

A solution of 35.5 g (0.50 mol) of methoxyacetonitrile in 29 ml (23 g, 0.50 mol) of ethanol and 30 ml of absolute diethylether was cooled to 0° C. and over 1 hour 22.5 g (0.62 mol) of hydrogen chloride gas was introduced, whilst towards the end of the introduction of gas the reaction product crystallised out. To complete the precipitation 130 ml of diethylether were added and the colourless needles were filtered off.

후처리

  1. additionwas introduced, whilst towards the end of the introduction of gas the reaction product
  2. customcrystallised out
  3. customthe precipitation 130 ml of diethylether
  4. additionwere added
  5. filtrationthe colourless needles were filtered off

출처 및 근거

ORD 기록
ord-a52066071dfd4d80a5ea89aab03b1819
출처 데이터셋
uspto-grants-2002_10
특허 번호
US06469039B1

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