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HRID1003508

反应详情

EQUATION

反应方程式

HRID 1003508 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：NCc1ccc2c(c1)OCO2
HCID75799

Benzo-1,3-dioxole-5-methylamine

C8H9NO2

结构：Clc1ccc2nc(Cl)nc(Cl)c2c1
HCID10421510

2,4,6-trichloroquinazoline

C8H3Cl3N2

PRODUCTS

生成物

1
结构：Clc1ccc2nc(Cl)nc(NCc3ccc4c(c3)OCO4)c2c1
HCID22339865

未命名化合物

收率 98%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

A mixture comprising 3.6 g of 2,4,6-trichloroquinazoline, 2.4 g of piperonylamine, 1.6 g of triethylamine and 50 ml of isopropyl alcohol was heated under reflux for 1.5 hours and hot-filtered to give 5.2 g of the title compound as a filter cake.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureunder reflux for 1.5 hours
  3. filtrationhot-filtered