HRID1003509

反应详情

EQUATION

反应方程式

HRID 1003509 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

35 ml of isopropyl alcohol, 900 mg of triethylamine and 1.35 g of piperonylamine were added to 2 g of 2,4-dichloro-6-cyanoquinazoline. The obtained mixture was heated under reflux for 1.5 hours and hot-filtered to recover a precipitate. Thus, 2.4 g of the title compound was obtained.

WORKUP

后处理

  1. temperatureThe obtained mixture was heated
  2. temperatureunder reflux for 1.5 hours
  3. filtrationhot-filtered
  4. customto recover a precipitate