Hydrochloric Acid → HCID 22666549, compound

HRID 1007892Notes

Reaction equation

HRID 1007892 reaction equation
[CH3:1][N:2]([CH3:18])[CH2:3][CH2:4][O:5][CH2:6][CH2:7][C:8]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH:11]=[CH:10][CH:9]=1.[ClH:19]>C(OCC)(=O)C>[ClH:19].[CH3:18][N:2]([CH3:1])[CH2:3][CH2:4][O:5][CH2:6][CH2:7][C:8]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH:11]=[CH:10][CH:9]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22666310HCID 22666310, compound

Product 1

HCID 22666549HCID 22666549, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent2×

Procedure

In 4.4 mL of ethyl acetate is dissolved 0.87 g of N,N-dimethyl-N-{2-[2-(1-naphthyl)ethoxy]ethyl}-amine, to which is added 1.3 mL of a 3.5 mol/L solution of dry hydrogen chloride in ethyl acetate. The resulting mixture is stirred at ambient temperature for one hour. The deposited crystal is collected by filtration, washed with ethyl acetate and dried to obtain 0.77 g of N,N-dimethyl-N-{2-[2-(1-naphthyl)ethoxy]ethyl}-amine hydrochloride.

Workup

  1. filtrationThe deposited crystal is collected by filtration
  2. washwashed with ethyl acetate
  3. customdried

Sources & evidence

ORD record
ord-bedf5223766946b38ee56d33855c7248
Source dataset
uspto-grants-2004_09
Patent number
US06797726B1

Reaction notes

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