HRID1010504

反应详情

EQUATION

反应方程式

HRID 1010504 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a 1 L flask equipped with a stirrer, a nitrogen introducing tube, a thermometer and a condenser, 50 g of stearyl acrylate, 49 g of n-butylacrylate, 1 g of hydroxyethyl acrylate, 0.89 g of AIBN, 100 mL of toluene and 100 mL of ethyl acetate were added and subjected to polymerization reaction in a stream of nitrogen at 70° C. for 12 hr, to obtain a copolymer of stearyl acrylate, n-butyl acrylate and hydroxyacrylate (hereinafter sometimes referred to “PSABAHEA”. The resulting PSABAHEA had a weight average molecular weight of 170,000.

WORKUP

后处理

  1. customTo a 1 L flask equipped with a stirrer, a nitrogen introducing tube
  2. customsubjected to polymerization reaction in a stream of nitrogen at 70° C. for 12 hr