HRID1010796
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The compound (B) (100 mg) was mixed with 3-Bromopropanol (120 mg) and K2CO3 (120 mg) in Acetonitrile. The reaction was refluxed overnight and filtered; the filtrate was evaporated and purified on silica gel column to give the titled product. Mass: (M+1), 214
WORKUP
后处理
- temperatureThe reaction was refluxed overnight
- filtrationfiltered
- customthe filtrate was evaporated
- custompurified on silica gel column