HRID1010796

反应详情

EQUATION

反应方程式

HRID 1010796 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The compound (B) (100 mg) was mixed with 3-Bromopropanol (120 mg) and K2CO3 (120 mg) in Acetonitrile. The reaction was refluxed overnight and filtered; the filtrate was evaporated and purified on silica gel column to give the titled product. Mass: (M+1), 214

WORKUP

后处理

  1. temperatureThe reaction was refluxed overnight
  2. filtrationfiltered
  3. customthe filtrate was evaporated
  4. custompurified on silica gel column